Synthesis of manganese titanate MnTiO3 powders by a sol-gel-hydrothermal method

被引:51
作者
Song, ZQ [1 ]
Wang, SB [1 ]
Yang, W [1 ]
Li, M [1 ]
Wang, H [1 ]
Yan, H [1 ]
机构
[1] Beijing Univ Technol, Coll Mat Sci & Engn, Beijing 100022, Peoples R China
来源
MATERIALS SCIENCE AND ENGINEERING B-SOLID STATE MATERIALS FOR ADVANCED TECHNOLOGY | 2004年 / 113卷 / 02期
关键词
MnTiO3; sol-gel-hydrothermal method; electronic properties;
D O I
10.1016/j.mseb.2004.06.002
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Manganese titanate (MnTiO3) powders have been synthesized by a sol-gel-hydrothermal method at low temperature below to 473 K through using NaOH as mineralizer. The structural character of as-synthesized powders were characterized by X-ray diffraction (XRD), scanning electron microscope (SEM), Fourier transformed infrared spectroscopy (FTIR) and Raman spectroscopy. The results indicate that the as-obtained powders are phase pure pyrophanite MnTiO3 with pie-shape morphology. The electronic properties of as-synthesized powders was characterized by UV-vis diffuse reflectance spectroscopy (UV-vis), which shows the as-obtained sample has a significant absorption in the visible region. (C) 2004 Elsevier B.V. All rights reserved.
引用
收藏
页码:121 / 124
页数:4
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