The effect of calcination and zirconia addition on HAp hot pressed materials

被引:14
作者
Brzezinska-Miecznik, Jadwiga [1 ]
Macherzynska, Beata [1 ]
Lach, Radoslaw [1 ]
Nowak, Barbara [1 ]
机构
[1] AGH Univ Sci & Technol, Krakow, Poland
关键词
Composites; Hydroxyapatite; Zirconia; HYDROXYAPATITE; COMPOSITES; HYDROXYLAPATITE; BEHAVIOR;
D O I
10.1016/j.ceramint.2014.07.108
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
081705 [工业催化]; 082905 [生物质能源与材料];
摘要
The effect of 5 and 10 vol% additives of zirconia (3Y TOSOH) to hydroxyapatite of natural origin was investigated. Two types of powders were applied; one prepared by mechanical mixing of constituents and the other by calcination at 900 degrees C of such mixtures followed by their milling. Calcined powders lead to the lower level of hydroxyapatite decomposition during hot pressing at 1200 degrees C. Hydroxyapatite, cubic zirconia and beta-TCP (beta-Ca-3(PO4)(2)) were found in the composites. Essential improvement of hardness, fracture toughness and mechanical strength compared to HAp matrix properties occurred. In the case of the material with 10 vol% zirconia additive the preliminary calcination of the starting powder resulted in better properties than in the case of the as-received powder. (C) 2014 Elsevier Ltd and Techna Group S.r.l. All rights reserved.
引用
收藏
页码:15815 / 15819
页数:5
相关论文
共 30 条
[1]
Adolfsson E., 2000, J AM SOC, V83, P27798
[2]
Mechanical characteristics of porous hydroxyapatite/oxide composites produced by post-sintering hot isostatic pressing [J].
Auger, M. A. ;
Savoini, B. ;
Munoz, A. ;
Leguey, T. ;
Monge, M. A. ;
Pareja, R. ;
Victoria, J. .
CERAMICS INTERNATIONAL, 2009, 35 (06) :2373-2380
[3]
Physiochemical characterizations of hydroxyapatite extracted from bovine bones by three different methods: Extraction of biologically desirable HAp [J].
Barakat, Nasser A. M. ;
Khalil, K. A. ;
Sheikh, Faheem A. ;
Omran, A. M. ;
Gaihre, Babita ;
Khil, Soeb M. ;
Kim, Hak Yong .
MATERIALS SCIENCE & ENGINEERING C-BIOMIMETIC AND SUPRAMOLECULAR SYSTEMS, 2008, 28 (08) :1381-1387
[4]
Brzezinska-Miecznik J., 2011, P 12 C EUR CER SOC E
[5]
Effect of zirconia addition on the microstructural evolution of porous hydroxyapatite [J].
Chiu, Chin-Yi ;
Hsu, Hsiu-Ching ;
Tuan, Wei-Hsing .
CERAMICS INTERNATIONAL, 2007, 33 (05) :715-718
[6]
Hot-pressed hydroxylapatite/monoclinic zirconia composites with improved mechanical properties [J].
Evis, Zafer ;
Doremus, Robert H. .
JOURNAL OF MATERIALS SCIENCE, 2007, 42 (07) :2426-2431
[7]
Reactions in hydroxylapatite-zirconia composites [J].
Evis, Zafer .
CERAMICS INTERNATIONAL, 2007, 33 (06) :987-991
[8]
Preparation and bioactivity evaluation of bone-like hydroxyapatite nanopowder [J].
Fathi, M. H. ;
Hanifi, A. ;
Mortazavi, V. .
JOURNAL OF MATERIALS PROCESSING TECHNOLOGY, 2008, 202 (1-3) :536-542
[9]
Effect of the calcination temperature on the composition and microstructure of hydroxyapatite derived from human and animal bone [J].
Figueiredo, M. ;
Fernando, A. ;
Martins, G. ;
Freitas, J. ;
Judas, F. ;
Figueiredo, H. .
CERAMICS INTERNATIONAL, 2010, 36 (08) :2383-2393
[10]
Gören S, 2004, KEY ENG MAT, V264-268, P1949