Alternative and mild procedures for the removal of organotin residues from reaction mixtures

被引：54

作者：

Renaud, P ^{[1
]}

Lacôte, E ^{[1
]}

Quaranta, L ^{[1
]}

机构：

[1] Univ Fribourg, Inst Chim Organ, CH-1700 Fribourg, Switzerland

来源：

TETRAHEDRON LETTERS | 1998年 / 39卷 / 15期

关键词：

D O I：

10.1016/S0040-4039(98)00066-5

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Simple treatment of tributyltin halide-containing reaction mixtures with Me3Al or aq. IM NaOH leads after filtration through silica gel to complete removal of tin residues. The Me3Al method is particularly convenient for polar products and the NaOH method for non-polar products. (C) 1998 Elsevier Science Ltd. All rights reserved.

引用

页码：2123 / 2126

页数：4

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