Continuous-flow preparation of biodiesel using microwave heating

被引:164
作者
Barnard, T. Michael
Leadbeater, Nicholas E. [1 ]
Boucher, Matthew B.
Stencel, Lauren M.
Wilhite, Benjamin A.
机构
[1] Univ Connecticut, UCONN Biofuels Consortium, Storrs, CT 06269 USA
[2] CEM Corp, Matthews, NC 28106 USA
关键词
D O I
10.1021/ef0606207
中图分类号
TE [石油、天然气工业]; TK [能源与动力工程];
学科分类号
0807 ; 0820 ;
摘要
The continuous-flow preparation of biodiesel using a commercially available scientific microwave apparatus offers a fast, easy route to this valuable biofuel. The methodology allows for the reaction to be run under atmospheric conditions and performed at flow rates of up to 7.2 L/min using a 4 L reaction vessel. It can be utilized with new or used vegetable oil with methanol and a 1:6 molar ratio of oil/alcohol. Energy consumption calculations suggest that the continuous-flow microwave methodology for the transesterification reaction is more energy-efficient than using a conventional heated apparatus.The continuous-flow preparation of biodiesel using a commercially available scientific microwave apparatus offers a fast, easy route to this valuable biofuel. The methodology allows for the reaction to be run under atmospheric conditions and performed at flow rates of up to 7.2 L/min using a 4 L reaction vessel. It can be utilized with new or used vegetable oil with methanol and a 1:6 molar ratio of oil/alcohol. Energy consumption calculations suggest that the continuous-flow microwave methodology for the transesterification reaction is more energy-efficient than using a conventional heated apparatus.
引用
收藏
页码:1777 / 1781
页数:5
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