Preparation of CexZr1-xO2 powders by microwave-induced combustion process

被引:36
作者
Fu, YP [1 ]
Lin, CH [1 ]
机构
[1] Natl Tsing Hua Univ, Dept Mat Sci & Engn, Hsinchu 300, Taiwan
关键词
ceria-zirconia; solid solution powders; combustion process;
D O I
10.1016/S0925-8388(03)00004-5
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
Ceria-zirconia solid solution powders were successfully synthesized by a microwave-induced combustion process. For the preparation, cerium nitrate, zirconyl nitrate dihydrate, and urea were used for the microwave-induced combustion process. The process took only a few minutes to obtain CexZr1-xO2 powders. The resultant powders were investigated by TG/DTA, XRD, TEM, and a surface area measurement. The as-received CexZr1-xO2 powders showed that the average particle size ranged from 10 to 20 nm, and the specific surface area was distributed from 40 to 50 m(2)/g. (C) 2003 Elsevier Science B.V. All rights reserved.
引用
收藏
页码:232 / 235
页数:4
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