Optimisation of alachlor solid-phase microextraction from water samples using experimental design

被引：27

作者：

González-Barreiro, C ^{[1
]}

Lores, M ^{[1
]}

Casais, MC ^{[1
]}

Cela, R ^{[1
]}

机构：

[1] Univ Santiago de Compostela, Fac Chem, Dept Analyt Chem, Santiago, Spain

来源：

JOURNAL OF CHROMATOGRAPHY A | 2000年 / 896卷 / 1-2期

关键词：

factorial design; experimental design; water analysis; alachlor; pesticides;

D O I：

10.1016/S0021-9673(00)00679-8

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

We have tested screening and response surface experimental designs to optimise the solid-phase microextraction (SPME) of the widely used herbicide alachlor. Extraction time and sample volume were the only statistically significant factors from those studied. In the final optimised conditions the procedure was applied to the SPME-HPLC analysis of alachlor in spiked water samples with excellent figures of merit. (C) 2000 Elsevier Science B.V. All rights reserved.

引用

页码：373 / 379

页数：7

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