A room temperature process for making Mn2O3 nano-particles and γ-MnOOH nano-rods

被引：22

作者：

Chandra, Navin ^{[1
]}

Bhasin, Sanjeev ^{[1
]}

Shanna, Meenakshi ^{[1
]}

Pal, Deepti ^{[1
]}

机构：

[1] CSIR, Reg Res Lab, Bhopal 462026, MP, India

来源：

MATERIALS LETTERS | 2007年 / 61卷 / 17期

关键词：

nano-materials; Mn2O3; nano-particles; MnOOH nano-rods; room temperature synthesis; X-ray diffraction; microstructure; REDUCTION;

D O I：

10.1016/j.matlet.2006.12.024

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

Nano-size crystals of Mn2O3 and MnOOH have been prepared by a simple precipitation process using dilute aqueous solutions of manganese sulphate and ammonia in the presence of sodium lauryl sulphate - a surface active agent. X-ray diffraction spectrometry has been used to identify the phases and to calculate the size of the nano-size crystals using the Scherrer method. The morphology of the crystals has been studied by TEM/ HRTEM and Edax has been used to estimate their elemental constituents. The sonication of the prepared nano-size material in acetone leads to the conversion of MnOOH to nano-sized Mn2O3. (c) 2006 Elsevier B.V. All rights reserved.

引用

页码：3728 / 3732

页数：5

共 17 条

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