Microwave synthesis of AgBiS2 dendrites in aqueous solution

被引：48

作者：

Chen, D ^{[1
]}

Shen, GZ ^{[1
]}

Tang, KB ^{[1
]}

Jiang, X ^{[1
]}

Huang, LY ^{[1
]}

Jin, Y ^{[1
]}

Qian, YT ^{[1
]}

机构：

[1] Univ Sci & Technol China, Dept Chem & Struct Res Lab, Hefei 230026, Peoples R China

来源：

INORGANIC CHEMISTRY COMMUNICATIONS | 2003年 / 6卷 / 06期

关键词：

microwave synthesis; dendritic crystals; alpha-AgBiS2; X-ray diffraction;

D O I：

10.1016/S1387-7003(03)00088-1

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

The microwave-assisted synthesis is generally much faster, cleaner, and more economical than the conventional methods. Here, dendritic crystals of AgBiS2 were synthesized in aqueous solution under microwave irradiation for 30 min. Powder X-ray diffraction (XRD) pattern indicates that the product is in the pure cubic phase. The product is also characterized by the techniques of transmission electron microscopy (TEM) and selected area electron diffraction (SAED). (C) 2003 Elsevier Science B.V. All rights reserved.

引用

页码：710 / 712

页数：3

共 13 条

[1] CHARACTERISTICS OF GRANULATED CATALYSTS FOR HYDROTREATING RAW LUBE STOCKS [J].

ALIEV, NM ;

ALIEV, VS ;

KASIMOV, AA ;

BABAEV, IM .

CHEMISTRY AND TECHNOLOGY OF FUELS AND OILS, 1992, 28 (5-6) :329-331

[2]

[Anonymous], 1967, Mineralium Deposita

[3] STANDARD ENTHALPIES OF FORMATION OF SULFIDES AND SULFOSALTS IN THE AG-BI-S SYSTEM BY HIGH-TEMPERATURE, DIRECT SYNTHESIS CALORIMETRY [J].

BRYNDZIA, LT ;

KLEPPA, OJ .

ECONOMIC GEOLOGY, 1988, 83 (01) :174-181

[4] PREPARATION AND STUDY OF SULFIDE THIN-FILMS DEPOSITED BY THE DIP TECHNIQUE [J].

KARANJAI, MK ;

DASGUPTA, D .

THIN SOLID FILMS, 1987, 155 (02) :309-315

[5]

KULLERUD G, 1959, ECON GEOL, V54, P533

[6]

MOH GH, 1971, NEUES JB MINERAL H, V9, P405

[7]

SASKIA AG, 1997, CHEM SOC REV, V26, P233

[8]

SHARAF KA, 1996, FIZIKA ZAGREB, V23, P932

[9]

SNMANTA LK, 1994, PHYS STATUS SOLIDI B, V182, P85

[10] SOL-GEL PREPARATION AND OPTICAL-PROPERTIES OF SILICA GLASSES CONTAINING CD AND ZN CHALCOGENIDE MICROCRYSTALS [J].

TOHGE, N ;

ASUKA, M ;

MINAMI, T .

JOURNAL OF NON-CRYSTALLINE SOLIDS, 1992, 147 :652-656

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