Structure solution with three-dimensional sets of precessed electron diffraction intensities

被引：57

作者：

Gemmi, Mauro

Nicolopoulos, Stavros

机构：

[1] Univ Milan, Dipartimento Sci Terra A Desio, I-20133 Milan, Italy

[2] Univ Politecn Valencia, Valencia 46022, Spain

[3] Nanomegas Sprl, B-1080 Brussels, Belgium

来源：

ULTRAMICROSCOPY | 2007年 / 107卷 / 6-7期

关键词：

electron diffraction; precession technique; electron crystallography; mineralogy;

D O I：

10.1016/j.ultramic.2006.03.010

中图分类号：

TH742 [显微镜];

学科分类号：

摘要：

The use of the precession technique for obtaining three-dimensional (3D) sets of electron diffraction intensities suitable for structure solution is discussed. The minerals uvarovite and Akermanite have been used as testing structures. The electron diffraction data sets obtained on these samples retain an acceptable linear relation with calculated structure factor amplitudes. The quality of these data is suitable to solve both structures using direct methods opening the possibility to use 3D precession ED data for solving unknown mineral structures. (c) 2006 Elsevier B.V. All rights reserved.

引用

页码：483 / 494

页数：12

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