A single-source approach to metastable Ni3S4 crystallites and their optical properties

被引：30

作者：

Chen, XY

Wang, ZH

Wang, X

Wan, JX

Liu, JW

Qian, YT ^{[1
]}

机构：

[1] Univ Sci & Technol China, Struct Res Lab, Anhua 230026, Peoples R China

[2] Univ Sci & Technol China, Dept Chem, Anhua 230026, Peoples R China

来源：

CHEMISTRY LETTERS | 2004年 / 33卷 / 10期

关键词：

D O I：

10.1246/cl.2004.1294

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Metastable Ni3S4 with good crystallinity has been firstly synthesized via a single-source approach using nickel diethyldithiocarbarnate as precursor under hydrothermal conditions. The optical properties of the as-prepared Ni3S4 are evaluated. It is found that the reaction temperature is of importance to the formation of Ni3S4 crystallites.

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页码：1294 / 1295

页数：2

相关论文

共 23 条

[1] Formation of crystalline stibnite bundles of rods by thermolysis of an antimony(III) diethyldithiocarbamate complex in ethylene glycol [J].

An, CH ;

Tang, KB ;

Yang, Q ;

Qian, YT .

INORGANIC CHEMISTRY, 2003, 42 (24) :8081-8086

[2] Solventless synthesis of nickel sulfide nanorods and triangular nanoprisms [J].

Ghezelbash, A ;

Sigman, MB ;

Korgel, BA .

NANO LETTERS, 2004, 4 (04) :537-542

[3] Nickel sulfide synthesized by ball milling as an attractive cathode material for rechargeable lithium batteries [J].

Han, SC ;

Kim, HS ;

Song, MS ;

Kim, JH ;

Ahn, HJ ;

Lee, JY .

JOURNAL OF ALLOYS AND COMPOUNDS, 2003, 351 (1-2) :273-278

[4] Synthesis of novel nickel sulfide submicrometer hollow spheres [J].

Hu, Y ;

Chen, JF ;

Chen, WM ;

Lin, XH ;

Li, XL .

ADVANCED MATERIALS, 2003, 15 (09) :726-729

[5] Synthesis of nickel sulfides in aqueous solutions using sodium dithionite [J].

Jeong, YU ;

Manthiram, A .

INORGANIC CHEMISTRY, 2001, 40 (01) :73-77

[6]

Jiang XC, 2001, ADV MATER, V13, P1278, DOI 10.1002/1521-4095(200108)13:16<1278::AID-ADMA1278>3.0.CO

[7]

2-W

[8] MARTENSITIC TOUGHENING OF CERAMICS [J].

KRIVEN, WM .

MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 1990, 127 (02) :249-255

[9] THE NI-S SYSTEM AND RELATED MINERALS [J].

KULLERUD, G ;

YUND, RA .

JOURNAL OF PETROLOGY, 1962, 3 (01) :126-175

[10]

LUNQVIST D, 1947, ARK KEMI MINERAL G A, V24, P21