A MAS NMR method for measuring 13C-17O distances

被引：91

作者：

Chopin, L

Vega, S ^{[1
]}

Gullion, T

机构：

[1] Weizmann Inst Sci, Dept Chem Phys, IL-76100 Rehovot, Israel

[2] Florida State Univ, Dept Chem, Tallahassee, FL 32306 USA

[3] W Virginia Univ, Dept Chem, Morgantown, WV 26506 USA

来源：

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY | 1998年 / 120卷 / 18期

关键词：

D O I：

10.1021/ja9732183

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Results of C-13,O-17-rotational-echo, double-resonance NMR (REDOR) and C-13,O-17-rotational-echo, adiabatic-passage, double-resonance NMR (REAPDOR) experiments on asparagine monohydrate are reported. The measurement of carbon-oxygen distances in a solid sample with magic-angle spinning NMR and O-17-enriched water is illustrated. These results show that determining the relative location of bound water in solids is possible and suggest that measuring distances between spin-1/2 nuclei and other chemical types of oxygen is feasible.

引用

页码：4406 / 4409

页数：4

共 27 条

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