Isotropic and anisotropic chemical shift in 207Pb NMR of inorganic solids

被引：4

作者：

Fayon, F ^{[1
]}

Bessada, C

Massiot, D

Farnan, I

Coutures, JP

机构：

[1] CNRS, Ctr Rech Phys Hautes Temp, F-45071 Orleans 2, France

[2] Univ Cambridge, Dept Earth Sci, Cambridge CB2 3EQ, England

来源：

JOURNAL DE CHIMIE PHYSIQUE ET DE PHYSICO-CHIMIE BIOLOGIQUE | 1998年 / 95卷 / 02期

关键词：

NMR; Pb-207; chemical shift; correlation;

D O I：

10.1051/jcp:1998138

中图分类号：

Q5 [生物化学]; Q7 [分子生物学];

学科分类号：

071010 ; 081704 ;

摘要：

We have recently described empirical correlations between Pb-207 NMR chemical shift (oxidation state 2+) and structure in solids (Fayon et al.) that should allow the use of Pb-207 NMR as a structural probe in disordered solids of complex composition. These empirical correlations are compared to new experimental NMR data in crystalline lead aluminates and lead silicates.

引用

页码：317 / 321

页数：5

共 9 条

[1] Empirical correlations between Pb-207 NMR chemical shifts and structure in solids
Fayon, F
Farnan, I
Bessada, C
Coutures, J
Massiot, D
Coutures, JP
[J]. JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1997, 119 (29) : 6837 - 6843
[2] SIDEBAND INTENSITIES IN NMR-SPECTRA OF SAMPLES SPINNING AT THE MAGIC ANGLE
HERZFELD, J
BERGER, AE
[J]. JOURNAL OF CHEMICAL PHYSICS, 1980, 73 (12) : 6021 - 6030
[3] SOLID-STATE PB-207 CP-MAS NMR OF LEAD(II) COMPOUNDS FOR THE STRUCTURAL STUDY OF MOLECULAR ROUTES TO LEAD-BASED PEROVSKITE-PHASE MATERIALS
IRWIN, AD
CHANDLER, CD
ASSINK, R
HAMPDENSMITH, MJ
[J]. INORGANIC CHEMISTRY, 1994, 33 (06) : 1005 - 1006
[4] NMR IN LEAD-CONTAINING COMPOUNDS
KIM, KS
BRAY, PJ
[J]. JOURNAL OF MAGNETIC RESONANCE, 1974, 16 (02) : 334 - 338
[5] CONVENTIONS FOR THE REPORTING OF NUCLEAR MAGNETIC SHIELDING (OR SHIFT) TENSORS SUGGESTED BY PARTICIPANTS IN THE NATO ARW ON NMR SHIELDING CONSTANTS AT THE UNIVERSITY-OF-MARYLAND, COLLEGE-PARK, JULY 1992
MASON, J
[J]. SOLID STATE NUCLEAR MAGNETIC RESONANCE, 1993, 2 (05) : 285 - 288
[6] Determination of Pb-207(2+) chemical shift tensors from precise powder lineshape analysis
Neue, G
Dybowski, C
Smith, ML
Hepp, MA
Perry, DL
[J]. SOLID STATE NUCLEAR MAGNETIC RESONANCE, 1996, 6 (03) : 241 - 250
[7] NMR CHEMICAL SHIFTS OF PB-207 IN A FEW COMPOUNDS
PIETTE, LH
WEAVER, HE
[J]. JOURNAL OF CHEMICAL PHYSICS, 1958, 28 (04) : 735 - 736
[8] CORRELATION OF SI-O-SI OR SI-O-AL ANGLES AND SI-29 NMR CHEMICAL-SHIFTS IN SILICATES AND ALUMINOSILICATES - INTERPRETATION BY SEMI-EMPIRICAL QUANTUM-CHEMICAL CONSIDERATIONS
RADEGLIA, R
ENGELHARDT, G
[J]. CHEMICAL PHYSICS LETTERS, 1985, 114 (01) : 28 - 30
[9] STRUCTURE AND CATION EFFECTS ON P-31 NMR CHEMICAL-SHIFTS AND CHEMICAL-SHIFT ANISOTROPIES OF ORTHO-PHOSPHATES
TURNER, GL
SMITH, KA
KIRKPATRICK, RJ
OLDFIELD, E
[J]. JOURNAL OF MAGNETIC RESONANCE, 1986, 70 (03): : 408 - 415

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