Application spectrum and data quality of the time-of-flight neutron diffractometer ROTAX at ISIS

被引:28
作者
Kockelmann, W [1 ]
Weisser, M
Heinen, H
Kirfel, A
Schäfer, W
机构
[1] Univ Bonn, Mineral Petrol Inst, DE-53115 Bonn, Germany
[2] Rutherford Appleton Lab, ISIS Facil, Chilton OX11 0QX, England
[3] Univ Wurzburg, Inst Mineral, DE-97070 Wurzburg, Germany
来源
EUROPEAN POWDER DIFFRACTION, PTS 1 AND 2 | 2000年 / 321-3卷
关键词
neutron diffraction; powder diffractometer; data precision; accuracy; texture analysis;
D O I
10.4028/www.scientific.net/MSF.321-324.332
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
The time-of-flight neutron diffractometer ROTAX at the pulsed spallation source ISIS is designed as a user instrument for diffraction studies of crystal and magnetic structures of predominantly polycrystalline samples. The multipurpose instrument can also be setup and operated as a texture diffractometer to collect complete pole figures of metallic and geological specimens. The instrument benefits from a wide d-spacing coverage (0.2 to 50 Angstrom), from high resolution at low d-spacings, and from a modular and flexible diffractometer setup. Results of recent performance tests are presented which were carried out to assess the quality of the ROTAX powder diffraction data and results. Present use and potential new applications of the user instrument are discussed.
引用
收藏
页码:332 / 337
页数:6
相关论文
共 14 条
[1]   X-RAY CHARGE-DENSITY STUDY OF RUTILE (TIO2) [J].
GONSCHOREK, W .
ZEITSCHRIFT FUR KRISTALLOGRAPHIE, 1982, 160 (3-4) :187-203
[2]  
*ISIS 98, 1998, RALTR1998050 ISIS CL
[3]  
JANSEN W, 1996, TEXTURES MICROSTR, V26, P11
[4]  
KEK HG, 1996, HASYLAB ANN REPORT, P664
[5]  
KOCKELMANN H, 1997, RALREPORTTR97018
[6]  
LARSON RB, 1994, GSAS GEN STRUCTURE A
[7]  
PALACIOS J, COMMUNICATION
[8]   SETUP AND USE OF THE ROTAX INSTRUMENT AT ISIS AS ANGLE-DISPERSIVE NEUTRON POWDER AND TEXTURE DIFFRACTOMETER [J].
SCHAFER, W ;
JANSEN, E ;
SKOWRONEK, R ;
WILL, G ;
KOCKELMANN, W ;
SCHMIDT, W ;
TIETZEJAENSCH, H .
NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION A-ACCELERATORS SPECTROMETERS DETECTORS AND ASSOCIATED EQUIPMENT, 1995, 364 (01) :179-185
[9]   Comparative diffraction experiments using monochromatic and pulsed white neutrons [J].
Schafer, W ;
Kockelmann, W ;
Jansen, E ;
Will, G .
PHYSICA B, 1997, 234 :1090-1092
[10]  
STEIGENBERGER U, 1997, 9762M ESS