Single crystal X-ray diffraction study of the spinel-type LiMn2O4

被引：66

作者：

Akimoto, J ^{[1
]}

Takahashi, Y ^{[1
]}

Gotoh, Y ^{[1
]}

Mizuta, S ^{[1
]}

机构：

[1] Natl Inst Mat & Chem Res, Tsukuba, Ibaraki 3058565, Japan

来源：

CHEMISTRY OF MATERIALS | 2000年 / 12卷 / 11期

关键词：

D O I：

10.1021/cm0003673

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

Single crystals of LiMn2O4 have been successfully synthesized for the first time. The single-crystal X-ray diffraction study confirmed the cubic spinel structure at 297 K. The structural phase transition around 285 K on the cooling process was confirmed by the single-crystal X-ray reciprocal space mapping method. Evidence of tripled periodicity toward the a and b axis directions has been observed at low temperatures.

引用

页码：3246 / +

页数：4

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