Cyclothreonine at 122K

被引：2

作者：

Anthoni, U ^{[1
]}

Fatum, TM ^{[1
]}

Flensburg, C ^{[1
]}

机构：

[1] Univ Copenhagen, Dept Chem, Ctr Crystallog Studies, DK-2100 Copenhagen, Denmark

来源：

ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS | 1998年 / 54卷

关键词：

D O I：

10.1107/S0108270197013887

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Spectroscopic and crystallographic data for the title compound (4S,5R)-4-amino-5-methyl-3-isoxazolidinone are reported. The title compound crystallizes with one half equivalent of water in a zwitterionic structure, C4H8N2O2.0.5H(2)O, stabilized by intermolecular hydrogen bonds.

引用

页码：240 / 242

页数：3

共 13 条

[1] Pseudomonine, an isoxazolidone with siderophoric activity from Pseudomonas fluorescens AH2 isolated from Lake Victorian Nile Perch [J].

Anthoni, U ;

Christophersen, C ;

Nielsen, PH ;

Gram, L ;

Petersen, BO .

JOURNAL OF NATURAL PRODUCTS, 1995, 58 (11) :1786-1789

[2]

Blessing R. H., 1987, Crystallogr. Rev, V1, P3, DOI [10.1080/08893118708081678, DOI 10.1080/08893118708081678]

[3]

Enraf-Nonius, 1989, CAD 4 SOFTW VERS 5 0

[4] ON ENANTIOMORPH-POLARITY ESTIMATION [J].

FLACK, HD .

ACTA CRYSTALLOGRAPHICA SECTION A, 1983, 39 (NOV) :876-881

[5] STRUCTURE AND REACTIONS OF CYCLOSERINE [J].

HIDY, PH ;

HODGE, EB ;

YOUNG, VV ;

HARNED, RL ;

BREWER, GA ;

PHILLIPS, WF ;

RUNGE, WF ;

STAVELY, HE ;

POHLAND, A ;

BOAZ, H ;

SULLIVAN, HR .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1955, 77 (08) :2345-2346

[6]

Johnson C. K., 1976, ORNL5138

[7] SYNTHESEN DES 4-AMINO-3-ISOXAZOLIDINONS (CYCLOSERIN) UND EINIGER ANALOGA [J].

PLATTNER, PA ;

BOLLER, A ;

FRICK, H ;

FURST, A ;

HEGEDUS, B ;

KIRCHENSTEINER, H ;

MAJNONI, S ;

SCHLAPFER, R ;

SPIEGELBERG, H .

HELVETICA CHIMICA ACTA, 1957, 40 (05) :1531-1552

[8]

PRETI C, 1979, J COORD COMPUT, V9, P25

[9]

Sheldrick G. M., 1996, SHELXL96 PROGRAM REF

[10] PHASE ANNEALING IN SHELX-90 - DIRECT METHODS FOR LARGER STRUCTURES [J].

SHELDRICK, GM .

ACTA CRYSTALLOGRAPHICA SECTION A, 1990, 46 :467-473

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