New cantharidinimides from cantharidin and 2-arylethylamines: Efficient synthesis under high pressure

被引:13
作者
Lin, PY [1 ]
Shi, SJ
Hsu, FL
Chen, CF
机构
[1] Taipei Med Coll, Sch Pharm, Taipei, Taiwan
[2] Natl Res Inst Chinese Med, Taipei, Taiwan
关键词
cantharidinimide; cantharidin; 2-arylethylamine;
D O I
10.1002/jccs.199800052
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
The new cantharidinimides 3a-j were prepared, in good to excellent yield, by heating the reactents 1 and 2a-j to 200 degrees C with toluene and triethylamine in a high pressure tube. The mixture was evaporated to dryness and furthermore heated to 180 degrees C-200 degrees C for 1 h.
引用
收藏
页码:323 / 326
页数:4
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