μ-aqua-pentaaqua[μ-3,6-bis(6-methyl-2-pyridyl)pyridazine]chlorodinickel(II) trichloride trihydrate

被引:5
作者
Sung, ND
Yun, KS
Kim, KG
Suh, IH [1 ]
机构
[1] Chungnam Natl Univ, Dept Phys, Taejon 305764, South Korea
[2] Chungnam Natl Univ, Div Appl Biol Chem, Taejon 305764, South Korea
来源
ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY | 2000年 / 56卷
关键词
D O I
10.1107/S0108270100010507
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
The title compound, mu-aqua-1:2 kappa(2)O-pentaaqua-1 kappa(2)O,2 kappa(3)O-mu-3,6-bis(6-methyl-2-pyridyl)pyridazine-1 kappa(2) N-1,N-6 :2 kappa(2)N(2),N-3-chloro-1 kappa Cl-dinickel(II) trichloride trihydrate, [Ni2Cl(C16H14N4)(H2O)(6)]Cl-3. 3H(2)O, consists of two Ni-II atoms, a 3,6-bis(6-methyl-2-pyridyl)pyridazine molecule, four Cl atoms and nine water molecules. The two Ni atoms are octahedrally coordinated by N and Cl atoms, and by water molecules, and the three six-membered rings, a pyridazine and two picolines, are planar to within 0.181 (3) Angstrom. The crystal structure is stabilized by an intra- and intermolecular hydrogen-bonding scheme involving water-water and water-chlorine interactions.
引用
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页码:E370 / E371
页数:2
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