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A review of oxygen-17 solid-state NMR of organic materials -: towards biological applications

被引：95
作者：
Lemaître, V
Smith, ME
Watts, A
机构：
[1] Univ Oxford, Dept Biochem, Biomembrane Struct Unit, Oxford OX1 3QU, England
[2] Nestec Ltd, BioAnalyt Dept, CH-1000 Lausanne 26, Switzerland
[3] Univ Warwick, Dept Phys, Coventry CV4 7AL, W Midlands, England
来源：
SOLID STATE NUCLEAR MAGNETIC RESONANCE | 2004年 / 26卷 / 3-4期
基金：
英国工程与自然科学研究理事会;
关键词：
oxygen-17; solid-state NMR; MAS; DOR; DAS; MQMAS; amino acids; organic molecules; peptide; hemeprotein; hydrogen-bond; biological applications; review;
D O I：
10.1016/j.ssnmr.2004.04.004
中图分类号：
O64 [物理化学（理论化学）、化学物理学];
学科分类号：
070304 ; 081704 ;
摘要：
O-17 solid state NMR of organic materials is developing rapidly. This article provides a snapshot of the current state of development of this field. The NMR techniques and enrichment protocols that are driving this progress are outlined. The O-17 parameters derived from solid-state NMR experiments are summarized and the structural sensitivity of the approach to effects such as hydrogen bonding highlighted. The prospects and challenges for O-17 solid-state NMR of biomolecules are discussed. (C) 2004 Elsevier Inc. All rights reserved.
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页码：215 / 235
页数：21
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