Crystal structure and thermal analysis of 1,5-diammonium-2-methyl pentane sulfate monohydrate

被引：6

作者：

Guerfel, T ^{[1
]}

Jouini, A ^{[1
]}

机构：

[1] Univ Ctr, Fac Sci Monastir, Dept Chim, Chim Solide Lab, Monastir 5000, Tunisia

来源：

JOURNAL OF CHEMICAL CRYSTALLOGRAPHY | 2000年 / 30卷 / 02期

关键词：

organic sulfate; crystal structure; DTA/TG/DSC;

D O I：

10.1023/A:1009561411167

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

Chemical preparation, x-ray single crystal, and thermal analysis of C6H18N2SO4. H2O (denoted DMPS) are described. The compound crystallizes in the triclinic system with P (1) over bar space group. Its unit cell dimensions are a = 5.826(1) Angstrom, b = 10.014(1) Angstrom, c = 11.221(1) Angstrom, alpha = 66.716(1)degrees beta = 84.395(1)degrees, gamma = 83.759(1)degrees, V = 596.7(1) Angstrom(3), and Z = 2. The DMPS structure is built up from inorganic chains parallel to the a axis and linked via O(W)-H ... O hydrogen bonds. These chains are interconnected by organic groups. Thermal analysis reveals the presence of one water molecule in the structure and shows a reversible weak phase transition.

引用

页码：95 / 98

页数：4

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