Effective and mild method for preparation of optically active α-amino aldehydes via TEMPO oxidation

被引：80

作者：

Jurczak, J

Gryko, D

Kobrzycka, E

Gruza, H

Prokopowicz, P

机构：

[1] Polish Acad Sci, Inst Organ Chem, PL-01224 Warsaw, Poland

[2] Univ Warsaw, Dept Chem, PL-02093 Warsaw, Poland

来源：

TETRAHEDRON | 1998年 / 54卷 / 22期

关键词：

D O I：

10.1016/S0040-4020(98)00299-3

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

The TEMPO oxidation method is successfully applied to preparation of variously protected, optically active a-amino aldehydes without racemization and in very good yield. (C) 1998 Elsevier Science Ltd. All rights reserved.

引用

页码：6051 / 6064

页数：14

共 31 条

[1] A GENERAL-METHOD OF ALPHA-AMINOALDEHYDE SYNTHESIS USING ALCOHOL-DEHYDROGENASE [J].

ANDERSSON, L ;

WOLFENDEN, R .

ANALYTICAL BIOCHEMISTRY, 1982, 124 (01) :150-157

[2]

ANELLI PL, 1987, J ORG CHEM, V52, P2559

[3]

[Anonymous], JANSEN CHIMICA ACTA

[4]

FUIJ N, 1995, J CHEM SOC P1, P1359

[5]

FUJII N, 1994, CHEM PHARM BULL, V42, P2241

[6] GLYCOSYL ALPHA-AMINO-ACIDS VIA STEREOCONTROLLED BUILDUP OF A PENALDIC ACID EQUIVALENT - A NOVEL SYNTHETIC APPROACH TO THE NUCLEOSIDIC COMPONENT OF THE POLYOXINS AND RELATED SUBSTANCES [J].

GARNER, P ;

PARK, JM .

JOURNAL OF ORGANIC CHEMISTRY, 1990, 55 (12) :3772-3787

[7] TOTAL SYNTHESIS OF PURPUROSAMINE-B FROM D-ALANINE [J].

GOLEBIOWSKI, A ;

JACOBSSON, U ;

RACZKO, J ;

JURCZAK, J .

JOURNAL OF ORGANIC CHEMISTRY, 1989, 54 (15) :3759-3760

[8] HIGH-PRESSURE APPROACH TO THE TOTAL SYNTHESIS OF 6-EPI-D-PURPUROSAMINE B [J].

GOLEBIOWSKI, A ;

JACOBSSON, U ;

JURCZAK, J .

TETRAHEDRON, 1987, 43 (13) :3063-3066

[9]

GOLEBIOWSKI A, 1993, POL J CHEM, V67, P685

[10]

GOLEBIOWSKI A, 1988, B POL ACAD SCI-CHEM, V36, P209

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