Microwave-assisted phenothiazines - Preparation by thionation of diphenylamines

被引：22

作者：

Filip, SV

Silberg, IA

Surducan, E

Vlassa, M

Surducan, V

机构：

[1] Inst Isotope & Mol Technol, Phys Mol Lab, RO-3400 Cluj Napoca 5, Romania

[2] Univ Babes Bolyai, Fac Chem & Chem Engn, Dept Organ Chem, RO-3400 Cluj Napoca, Romania

来源：

SYNTHETIC COMMUNICATIONS | 1998年 / 28卷 / 02期

关键词：

D O I：

10.1080/00397919808005727

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

A preparation in 'dry media' of phenothiazine derivatives by thionation of diphenylamines using microwave-activation is presented. This method allowed the preparation of 2,4,6,8-tetra-tert-butyl-10H-phenothiazine 2e, the first 2,4,6,8-tetra-substituted derivative of this heterocycle, practically inaccessible by other thionation procedure.

引用

页码：337 / 345

页数：9

共 26 条

[1] APPLICATION OF MICROWAVE-HEATING TECHNIQUES FOR THE SYNTHESIS OF SOLID-STATE INORGANIC-COMPOUNDS [J].