Application of electroseparation methods in beta-agonist drugs characterization

被引:9
作者
Efstatiade, MD
Baiulescu, GE
机构
[1] Department of Analytical Chemistry, Faculty of Chemistry, University of Bucharest, 70346 Bucharest 3
关键词
clenbuterol; salbutamol; terbutaline; pharmaceuticals; capillary zone electrophoresis; micellar electrokinetic chromatography;
D O I
10.1080/00032719708001819
中图分类号
O65 [分析化学];
学科分类号
070302 [分析化学]; 081704 [应用化学];
摘要
The possibility of using electroseparation methods with UV/Vis detection in the study of some beta-agonist drugs has been investigated. Clenbuterol, Salbutamol and Terbutaline were separated and quantitatively analyzed in various drugs. The influence of several parameters, such as pH, temperature, surfactants, column type and electrical values were studied. The electroseparation methods have shown good reproducibility, accuracy and short analysis time with a small sample preparation and low reagent consumption.
引用
收藏
页码:2755 / 2764
页数:10
相关论文
共 18 条
[1]
COMPARISON OF ISOTACHOPHORESIS, CAPILLARY ZONE ELECTROPHORESIS AND HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY FOR THE DETERMINATION OF SALBUTAMOL, TERBUTALINE SULFATE AND FENOTEROL HYDROBROMIDE IN PHARMACEUTICAL DOSAGE FORMS [J].
ACKERMANS, MT ;
BECKERS, JL ;
EVERAERTS, FM ;
SEELEN, IGJA .
JOURNAL OF CHROMATOGRAPHY, 1992, 590 (02) :341-353
[2]
DETERMINATION OF SALBUTAMOL-RELATED IMPURITIES BY CAPILLARY ELECTROPHORESIS [J].
ALTRIA, KD .
JOURNAL OF CHROMATOGRAPHY, 1993, 634 (02) :323-328
[3]
ALTRIA KD, 1993, LC GC N AM, V11, P438
[4]
APPLICATION OF AN ENZYME-LINKED-IMMUNOSORBENT-ASSAY KIT FOR BETA-AGONIST SCREENING OF BOVINE URINES IN NORTH-EASTERN ITALY [J].
ANGELETTI, R ;
ORIUNDI, MP ;
PIRO, R ;
BAGNATI, R .
ANALYTICA CHIMICA ACTA, 1993, 275 (1-2) :215-219
[5]
EFFECT OF SAMPLE STACKING ON RESOLUTION, CALIBRATION GRAPHS AND PH IN CAPILLARY ZONE ELECTROPHORESIS [J].
BECKERS, JL ;
ACKERMANS, MT .
JOURNAL OF CHROMATOGRAPHY, 1993, 629 (02) :371-378
[6]
DETERMINATION OF CLENBUTEROL RESIDUES BY LIQUID-CHROMATOGRAPHY ELECTROSPRAY MASS-SPECTROMETRY [J].
DEBRAUWER, L ;
BORIES, G .
ANALYTICA CHIMICA ACTA, 1993, 275 (1-2) :231-239
[7]
SCREENING AND CONFIRMATORY ANALYSIS OF BETA-AGONISTS, BETA-ANTAGONISTS AND THEIR METABOLITES IN HORSE URINE BY CAPILLARY GAS-CHROMATOGRAPHY MASS-SPECTROMETRY [J].
DUMASIA, MC ;
HOUGHTON, E .
JOURNAL OF CHROMATOGRAPHY-BIOMEDICAL APPLICATIONS, 1991, 564 (02) :503-513
[8]
EFFECTIVE LABORATORY MONITORING FOR THE ABUSE OF THE BETA-AGONIST CLENBUTEROL IN CATTLE [J].
ELLIOTT, CT ;
MCEVOY, JDG ;
MCCAUGHEY, WJ ;
SHORTT, DH ;
CROOKS, SRH .
ANALYST, 1993, 118 (04) :447-448
[9]
Garcia Regueiro J. A., 1993, Journal of Chromatography A, V655, P73, DOI 10.1016/0021-9673(93)87012-B
[10]
EXTRACTION AND CLEANUP OF THE BETA-AGONIST SALBUTAMOL FROM LIVER AND ITS DETERMINATION BY ENZYME-IMMUNOASSAY [J].
HOWELLS, L ;
SAUER, M ;
SAYER, R ;
CLARK, D .
ANALYTICA CHIMICA ACTA, 1993, 275 (1-2) :275-278