Structure and electrical properties of multilayer PZT films prepared by sol-gel processing

被引:17
作者
Miyazawa, K
Ito, K
Maeda, R
机构
[1] Univ Tokyo, Sch Engn, Dept Mat Sci, Bunkyo Ku, Tokyo 1138656, Japan
[2] Minist Int Trade & Ind, Agcy Ind Sci & Technol, Mech Engn Lab, Tsukuba, Ibaraki 305, Japan
关键词
D O I
10.1016/S0272-8842(99)00085-1
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Multilayer PZT(Zr:Ti = 52:48) films were prepared by the repeated process of spin-coating and firing at 600 degrees C of a PZT sol with various heating rates between 20 and 200 degrees C min(-1). Their structural and dielectric properties were examined. The multilayer film prepared with the heating rate of 50 degrees C min(-1) shows the highest dielectric constant and a smooth surface with no surface cracks. High-resolution TEM (HRTEM) observations of an as-deposited PZT film indicate nucleation of perovskite and pyrochlore crystals in the amorphous matrix. The perovskite crystals are found to form through the initial construction of {110} planes. (C) 2000 Elsevier Science Ltd acid Techna S.r.l. All rights reserved.
引用
收藏
页码:501 / 506
页数:6
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