Evaluation of the surface roughness of microporous Ni-Zn-P electrodes by in situ methods

被引:106
作者
Karimi Shervedani R. [1 ]
Lasia A. [1 ]
机构
[1] Département de Chimie, Université de Sherbrooke, Sherbrooke
关键词
CO oxidation; electrode capacitance; hydrogen evolution reaction; nickel based electrodes; surface roughness;
D O I
10.1023/A:1003577631897
中图分类号
学科分类号
摘要
The surface roughness of porous Ni-Zn-P electrodes was studied in 1 M NaOH using in situ electrochemical techniques: ratio of the polarization current densities, electrochemical impedance spectroscopy, cyclic voltammetry, coulometric oxidation of the surface, and a new technique of a CO molecular probe. The obtained surface roughness was about 5.5×103. Good agreement was observed between the results obtained by all these techniques.
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页码:979 / 986
页数:7
相关论文
共 23 条
[1]  
Trasatti, S., Petrii, O.A., (1991) Pure Appl. Chem., 63, p. 711
[2]  
Kuhn, A.T., (1987) Techniques in Electrochemistry, Corrosion and Metal Finishing, p. 95. , A.T. Kuhn (ed.) J. Wiley & Sons, Chichester
[3]  
Lasia, A., (1993) Current Topics Electrochem., 2, p. 239
[4]  
Gu, P., Bai, L., Brousseau, R., Conway, B.E., (1992) Electochim. Acta., 37, p. 2145
[5]  
Bai, L., Gao, L., Conway, B.E., (1993) J. Chem. Soc. Faraday Trans., 89, p. 235
[6]  
Šimpraga, R., Tremiliosi-Filho, G., Qian, S.Y., Conway, B.E., (1997) J. Electroanal. Chem., 424, p. 141
[7]  
Assunção, N.A., De Giz, M.J., Tremiliosi-Filho, G., Gonzalez, E.R., (1997) J. Electrochem. Soc., 144, p. 2794
[8]  
Rauch, S., Wendt, H., (1996) J. Electrochem. Soc., 143, p. 2852
[9]  
Machado, S.A.S., Tiengo, J., De Lima Neto, P., Avaca, L.A., (1994) Electrochim. Acta, 39, p. 1757
[10]  
Machado, S.A.S., Tiengo, J., De Lima Neto, P., Avaca, L.A., (1996) J. Appl. Electrochem., 26, p. 431