LEAD IN FEED INCIDENT - MULTIELEMENT ANALYSIS OF CATTLE FEED AND TISSUES BY INDUCTIVELY COUPLED PLASMA-MASS SPECTROMETRY AND COOPERATIVE QUALITY ASSURANCE SCHEME FOR LEAD ANALYSIS OF MILK

被引：13

作者：

CREWS, HM

BAXTER, MJ

BIGWOOD, T

BURRELL, JA

OWEN, LM

ROBINSON, C

WRIGHT, C

MASSEY, RC

机构：

[1] Food Science Laboratory, Food Safety Directorate, Ministry of Agriculture, Fisheries and Food, Norwich, NR4 7UQ, Norwich Research Park, Colney

来源：

FOOD ADDITIVES AND CONTAMINANTS | 1992年 / 9卷 / 04期

关键词：

LEAD; MULTIELEMENT; MICROWAVE DISSOLUTION; ICP-MS; CATTLE FEED; TISSUES; MILK; QUALITY ASSURANCE SCHEME;

D O I：

10.1080/02652039209374083

中图分类号：

O69 [应用化学];

学科分类号：

081704 ;

摘要：

Contaminated cattle feed was imported into the UK in 1989 and resulted in lead toxicity in some animals. Rapid analyses for lead and several other possible contaminating elements were required for feed and cattle tissues. Microwave dissolution of samples with measurement by ICP-MS was used for multi-element determinations. Lead was found to be the major contaminant. Lead levels in milk samples were measured by several laboratories during the crisis and an analytical quality assurance scheme was devised to monitor the quality of the data. The scheme allowed any poorly performing laboratories to be rapidly identified and excluded from the survey.

引用

页码：365 / 378

页数：14

共 19 条

[1]

Baars A.J., Van Beek H., Kisser I.J.R., Vos G., Van Delft W., Fennema G., Lieben G.W., Lautenbag K., Nieuwenhuiji J.H.M., De Lezenne Colander P.A., Pluimers F.H., Van De Haar G., Jorna T.J., Tuinstra L., Zandstra P., Bruins B., Lead intoxication in cattle in the northern part of the Netherlands, October 1989-January1990, Tijdschrift Voor Diergeneeskunde, 115, pp. 882-890, (1990)

[2]

Baxter M.J., Burrell J.A., Crews H.M., Smith A., Massey R.C., Leadcontamination during domestic preparation and cooking of potatoes and leaching of bonederivedlead on roasting, marinading and boiling beef, Food Additives and Contaminants, 9, pp. 225-235, (1992)

[3]

Brown S.S., Savory J., Chemical Toxicology and Clinical Chemistry of Metals, (1983)

[4]

Collery P., Poirier L.A., Manfait M., Etienne J.C., Metal Ions in Biology And, (1990)

[5]

Lead in Health, (1980)

[6]

Ernhart C.B., Scarr S., Childhood Lead Exposure, What Do We Know and How Do We, (1991)

[7]

Friel J.K., Skinner C.S., Jackson S.E., Longerich H.P., Analysis of biologicalreference materials, prepared by microwave dissolution, using inductively coupled plasma massspectrometry, Analyst, 115, pp. 269-273, (1990)

[8]

Lee W.R., Moore M.R., Low level exposure to lead, the evidence for harm accumulates, British Medical Journal, 201, pp. 504-506, (1990)

[9]

Mahaffey K.R., Nutritional factors in lead poisoning, Nutrition Reviews, 39, pp. 353-362, (1981)

[10]

Mertz W., Trace Elements in Human and Animal Nutrition, (1986)

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