HIGH-RESOLUTION GAS-CHROMATOGRAPHY MASS-SPECTROMETRY OF POLYCHLORINATED BIPHENYL CONGENERS IN BIOLOGICAL SAMPLES

被引：10

作者：

DRISS, MR

SABBAH, S

BOUGUERRA, ML

机构：

[1] FAC SCI TUNIS,DEPT CHIM,CAMPUS UNIV BELVEDERE,TUNIS 1060,TUNISIA

[2] INST NATL RECH SCI & TECH,HAMMAM LIF 2050,TUNISIA

来源：

JOURNAL OF CHROMATOGRAPHY | 1991年 / 552卷 / 1-2期

关键词：

D O I：

10.1016/S0021-9673(01)95936-9

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

A study is performed on polychlorinated biphenyl (PCB) congener residues in samples of human blood and milk as well as in falcon and pigeon eggs. Most of the PCB congeners found in these biological samples were quantified by high-resolution gas chromatography (HRGC). A PCB technical mixture -namely, DP6 (Phenochlor)- was used for the calibration as its composition was previously determined by HRGC-mass spectrometry. The usefulness of such a congener analysis is outlined. It is the first time to the best of our knowledge that a Phenochlor mixture is used for standardization.

引用

页码：213 / 222

页数：10

共 25 条

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[2] QUANTITATIVE CHARACTERIZATION OF POLYCHLORINATED BIPHENYL MIXTURES (AROCLOR-1248, AROCLOR-1254 AND AROCLOR-1260) BY GAS-CHROMATOGRAPHY USING CAPILLARY COLUMNS [J].