ENANTIOMERIC PURITY OF MOSHER ACID

被引：17

作者：

KONIG, WA

NIPPE, KS

MISCHNICK, P

机构：

[1] Institut für Organische Chemic, Universität Hamburg, D-2000 Hamburg 13

来源：

TETRAHEDRON LETTERS | 1990年 / 31卷 / 47期

关键词：

D O I：

10.1016/S0040-4039(00)97192-2

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Several commercial samples of 2-methoxy-2-phenyl-3,3,3-trifluoropropionic acid (Mosher's acid, MTPA) were investigated for enantiomeric purity by capillary gas chromatography with octakis(3-O-butyryl-2,6-di-O-pentyl)-γ-cyclodextrin as a chiral stationary phase. Enantiomeric purities were found between 97.89 % and 99.80 %. © 1990.

引用

页码：6867 / 6868

页数：2

共 6 条

[1] ALPHA-METHOXY-ALPHA-TRIFLUOROMETHYLPHENYLACETIC ACID, A VERSATILE REAGENT FOR DETERMINATION OF ENANTIOMERIC COMPOSITION OF ALCOHOLS AND AMINES [J].