ALPHA-METHOXY-ALPHA-(TRIFLUOROMETHYL)BENZYL ISOCYANATE - A CONVENIENT REAGENT FOR THE DETERMINATION OF THE ENANTIOMERIC COMPOSITION OF PRIMARY AND SECONDARY-AMINES

被引：20

作者：

NABEYA, A

ENDO, T

机构：

来源：

JOURNAL OF ORGANIC CHEMISTRY | 1988年 / 53卷 / 14期

关键词：

D O I：

10.1021/jo00249a044

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

引用

页码：3358 / 3361

页数：4

共 16 条

[1] ALPHA-METHOXY-ALPHA-TRIFLUOROMETHYLPHENYLACETIC ACID, A VERSATILE REAGENT FOR DETERMINATION OF ENANTIOMERIC COMPOSITION OF ALCOHOLS AND AMINES [J].

DALE, JA ;

DULL, DL ;

MOSHER, HS .

JOURNAL OF ORGANIC CHEMISTRY, 1969, 34 (09) :2543-&

[2] NUCLEAR MAGNETIC-RESONANCE ENANTIOMER REAGENTS - CONFIGURATIONAL CORRELATIONS VIA NUCLEAR MAGNETIC-RESONANCE CHEMICAL-SHIFTS OF DIASTEREOMERIC MANDELATE, O-METHYLMANDELATE, AND ALPHA-METHOXY-ALPHA-TRIFLUOROMETHYLPHENYLACETATE (MTPA) ESTERS [J].

DALE, JA ;

MOSHER, HS .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1973, 95 (02) :512-519

[3]

HINE J, 1962, PHYSICAL ORGANIC CHE, P336

[4] ISOMERIZATION OF 1-THIOACYLAZETIDINES AND RELATED COMPOUNDS [J].

IWAKURA, Y ;

NABEYA, A ;

NISHIGUC.T ;

OHKAWA, KH .

JOURNAL OF ORGANIC CHEMISTRY, 1966, 31 (10) :3352-&

[5] DETERMINATION OF ENANTIOMERIC PURITIES OF ALCOHOLS AND AMINES BY A P-31 NMR TECHNIQUE [J].

JOHNSON, CR ;

ELLIOTT, RC ;

PENNING, TD .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1984, 106 (17) :5019-5020

[6] A SIMPLE METHOD FOR DISTINGUISHING OPTICAL ISOMERS OF CHIRAL AMINES, HYDROXYLAMINES, AMINO-ACIDS, AND PEPTIDES [J].

KOLASA, T ;

MILLER, MJ .

JOURNAL OF ORGANIC CHEMISTRY, 1986, 51 (15) :3055-3058

[7] CONFIGURATION OF OPTICALLY-ACTIVE PHOSPHORUS THIO ACIDS .4. H-1, P-31, AND C-13 NUCLEAR MAGNETIC-RESONANCE NONEQUIVALENCE OF DIASTEREOMERIC SALTS OF CHIRAL PHOSPHORUS THIO ACIDS WITH OPTICALLY-ACTIVE AMINES - METHOD FOR DETERMINING OPTICAL PURITY AND CONFIGURATION OF CHIRAL PHOSPHORUS THIO ACIDSD [J].

MIKOLAJCZYK, M ;

OMELANCZUK, J ;

LEITLOFF, M ;

DRABOWICZ, J ;

EJCHART, A ;

JURCZAK, J .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1978, 100 (22) :7003-7008

[8]

Pirkle W.H., 1982, TOP STEREOCHEM, V13, P263

[9]

Pirkle W.H., 1979, J ORG CHEM, V44, P4891

[10] NUCLEAR MAGNETIC-RESONANCE DETERMINATION OF ENANTIOMERIC COMPOSITION AND ABSOLUTE-CONFIGURATION OF AMINES, ALCOHOLS, AND THIOLS WITH ALPHA-[1-(9-ANTHRYL)-2,2,2-TRIFLUOROETHOXY]ACETIC ACID AS A CHIRAL DERIVATIZING AGENT [J].

PIRKLE, WH ;

SIMMONS, KA .

JOURNAL OF ORGANIC CHEMISTRY, 1981, 46 (16) :3239-3246

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