STRUCTURAL ORDER IN MCM-41 CONTROLLED BY SHIFTING SILICATE POLYMERIZATION EQUILIBRIUM

被引:260
作者
RYOO, R [1 ]
KIM, JM [1 ]
机构
[1] KOREA ADV INST SCI & TECHNOL, CTR MOLEC SCI, TAEJON 305701, SOUTH KOREA
关键词
D O I
10.1039/c39950000711
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Powder X-ray diffraction, Si-29 and Xe-129 NMR spectroscopy of MCM-41 show that the long-range structural order and textural uniformity of the mesoporous molecular sieve are markedly improved due to a shift in the reaction equilibrium when acetic acid is repeatedly added during the conversion of sodium silicate and NMe(3)(C16H33)Cl to a MCM-41 phase.
引用
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页码:711 / 712
页数:2
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