NEW TECHNIQUE TO MEASURE THE TOUGHNESS OF THIN-FILM INTERFACES

被引:21
作者
GUPTA, V
PRONIN, A
机构
[1] Thayer School of Engineering, Dartmouth College, Hanover, New Hampshire
关键词
D O I
10.1111/j.1151-2916.1995.tb08503.x
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
A new technique to measure the toughness of metal-ceramic interfaces is presented, In this technique, a test coating of 100 to 200 Angstrom is deposited on the substrate of interest. This layer is then overlaid by a residually stressed Nb coating (used as a loading device), and its thickness is controlled until the lower test layer buckles away from the substrate. By determining the intrinsic residual strain within the Nb layer in independent delamination experiments, the bilayer buckling morphology is quantified, and a measure of the interface fracture toughness is obtained. This technique has been successfully applied to interfaces between metallic coatings of Sb, Cr, Cu, Nb, Al, and substrates of sapphire with (0001) orientation. Interface toughness values of 0.31, 0.94, 0.93, 0.88, and 1.0 J/m(2) were obtained for these systems, respectively.
引用
收藏
页码:1397 / 1400
页数:4
相关论文
共 8 条
[1]  
Yuan J., Gupta V., Measurement of Interface Strength by the Modified Laser Spallation Technique. Part I: Experimental Technique and Modeling the Spallation Process, J. Appl. Phys., 74, 4, pp. 2388-2396, (1993)
[2]  
Gupta V., Yuan J., Pronin A., Recent Developments in the Laser Spallation Technique to Measure the Interface Strength and Its Relationship to Interface Toughness with Applications to Metal/Ceramic, Ceramic/Ceramic and Ceramic/Polymer Interfaces, J. Adhes. Sci. Technol., 8, 6, pp. 713-747, (1994)
[3]  
Evans A.G., Ruhle M., Dalgleish B.J., Charalambides P.G., The Fracture Energy of Bimaterial Interfaces, Mater. Sci. Eng., 126 A, pp. 53-64, (1990)
[4]  
Argon A.S., Gupta V., Landis H.S., Cornie A., Intrinsic Toughness of Interfaces between SiC Coatings and Substrates of Si or C Fiber, J. Mater. Sci., 24, pp. 1207-1218, (1989)
[5]  
Hutchinson J.W., Suo Z., Mixed Mode Cracking in Layered Materials, Advances in Applied Mechanics, pp. 63-191, (1992)
[6]  
Bagchi A., Lucas G.E., Suo Z., Evans A.G., A New Procedure for Measuring the Decohesion Energy for Thin Ductile Films on Substrates, J. Mater. Res., 9, 7, pp. 1734-1741, (1994)
[7]  
Yuan J., Gupta V., Kim M., Structure and Chemistry of Nb/Sapphire Interfaces, with and without Interlayers of Sb and Cr, Acta Metall. Mater., 43, 2, pp. 769-779, (1995)
[8]  
Ortiz M., Gioio G., The Morphology and Folding Patterns of Buckling‐Driven Thin‐Film Blisters, J. Mech. Phys. Solids, 42, 3, pp. 531-559, (1994)