HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHIC ANALYSIS OF FLAVONOL GLYCOSIDES OF SOLIDAGO-VIRGAUREA

被引：16

作者：

PIETTA, P ^{[1
]}

GARDANA, C ^{[1
]}

MAURI, P ^{[1
]}

ZECCA, L ^{[1
]}

机构：

[1] CNR,IST TECNOL BIOMED AVANZATE,I-20131 MILAN,ITALY

来源：

JOURNAL OF CHROMATOGRAPHY | 1991年 / 558卷 / 01期

关键词：

D O I：

10.1016/0021-9673(91)80135-4

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

Solidago virgaurea flavonols were separated by reversed-phase high-performance liquid chromatography (RPLC) on a C-8 column using 2-propanol water (14:86) as eluent in the isocratic mode. The presence of rutin, kaempferol-3-O-rutinoside, kaempferol-3-O-robinobioside and isorhamnetin-3-O-rutinoside was confirmed. The identity of kaempferol-3-O-robinobioside was proved by acid hydrolysis followed by determination of kaempferol and rhamnose/galactose and mass spectrometry. A rapid isocratic separation of the flavonol aglycones obtained by acid hydrolysis of the Solidago virgaurea extract is also described.

引用

页码：296 / 301

页数：6

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