APPLICATION OF MICROWAVE-ENERGY TO ORGANIC-SYNTHESIS - IMPROVED TECHNOLOGY

被引：54

作者：

ABRAMOVITCH, RA

ABRAMOVITCH, DA

IYANAR, K

TAMARESELVY, K

机构：

[1] Department of Chemistry, Clemson University, Clemson

来源：

TETRAHEDRON LETTERS | 1991年 / 32卷 / 39期

关键词：

D O I：

10.1016/S0040-4039(00)92356-6

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

The application of microwave energy to the sulfonation of naphthalene and anthraquinone, to the amination of p-chloronitrobenzene, and to the hydrosilylation of 2- and 4-vinylpyridine has been studied. Though faster (5 - 360-fold) reactions were observed problems were encountered with the available microwave technology. These were overcome by using a microwave oven equipped with stirring facility and both temperature and pressure control.

引用

页码：5251 / 5254

页数：4

共 24 条

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