DETERMINATION OF PARTICLE DISTRIBUTION IN SUPPORTED METAL-CATALYSTS BY SMALL-ANGLE SCATTERING

被引：13

作者：

ESPINAT, D ^{[1
]}

MORAWECK, B ^{[1
]}

LARUE, JF ^{[1
]}

RENOUPREZ, AJ ^{[1
]}

机构：

[1] INST RECH CATALYSE,2 AVE ALBERT EINSTEIN,F-69626 VILLEURBANNE,FRANCE

来源：

JOURNAL OF APPLIED CRYSTALLOGRAPHY | 1984年 / 17卷 / AUG期

关键词：

CATALYSTS - X-Ray Analysis;

D O I：

10.1107/S0021889884011493

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

A method of processing X-ray small-angle data for a three-phase system, based on the hypothesis formulated by Goodisman, Brumberger & Cupelo has been extended to the determination of the polydispersity of one phase. For supported metal catalysts, the characterization of the metal phase is obtained from its correlation function evaluated from a balanced subtraction between those of the catalyst and of the support, measured in two separate experiments. A fairly good agreement with electron microscopy data is obtained.

引用

页码：269 / 272

页数：4

共 13 条

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