DEVELOPMENT OF THE SIMULTANEOUS THERMAL-ANALYSIS X-RAY-SCATTERING MEASUREMENT SYSTEM

被引:38
作者
YOSHIDA, H [1 ]
KINOSHITA, R [1 ]
TERAMOTO, Y [1 ]
机构
[1] SEIKO INSTRUMENTS LTD,DIV SCI INSTRUMENTS,OYA 41013,SHIZUOKA,JAPAN
关键词
DSC; THERMAL ANALYSIS; WIDE ANGLE X-RAY DIFFRACTOMETER; X-RAY SCATTERING;
D O I
10.1016/0040-6031(95)02326-W
中图分类号
O414.1 [热力学];
学科分类号
摘要
A new simultaneous DSC/X-ray measurement system was developed for the purpose of combining X-ray scattering data and calorimetric data. The DSC/X-ray measurement system was equipped with a conventional wide-angle X-ray diffractometer (WAXD). The phase transition behavior of pure hexatriacontane was measured by the DSC/WAXD, both on heating and cooling. The accuracy and reproducibility of the simultaneous DSC/X-ray instrument were comparable with the conventional DSC.
引用
收藏
页码:173 / 183
页数:11
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