CIMATEROL AND CLENBUTEROL RESIDUE ANALYSIS BY HPLC-HPTLC IN LIVER

被引：25

作者：

DEGROODT, JM

DEBUKANSKI, BW

DEGROOF, J

BEERNAERT, H

机构：

[1] Ministère de la Santé Publique et de l'Environnement, Brussels, B-1050, 14, rue J. Wytsman

来源：

ZEITSCHRIFT FUR LEBENSMITTEL-UNTERSUCHUNG UND-FORSCHUNG | 1991年 / 192卷 / 05期

关键词：

D O I：

10.1007/BF01193142

中图分类号：

TS2 [食品工业];

学科分类号：

0832 ;

摘要：

A method has been developed for the analysis of cimaterol and clenbuterol residues in liver, with detection limits of 0.25-mu-g/kg and 0.5-mu-g/kg, respectively. The recovery varied from 55% to 60%. After extraction, a clean-up procedure with Baker-spe C-18 columns was performed. The two chemical compounds of interest were eluted with methanol. Cimaterol and clenbuterol were quantitatively determined by high-performance liquid chromatography (HPLC) using an RP-Select B (5-mu-m) column and a post-column reaction procedure. The positive results were confirmed by high-performance thin-layer chromatography (HPTLC) as this technique reaches the same level of sensitivity as the HPLC method.

引用

页码：430 / 432

页数：3

共 11 条

[1]

Beermann D. H., 1986, In 'Proceedings of the 1986 Cornell nutrition conference for feed manufacturers' [see FSTA (1987) 19 4A8]., P29

[2] EFFECTS OF CIMATEROL AND FISH-MEAL ON PERFORMANCE, CARCASS CHARACTERISTICS AND SKELETAL-MUSCLE GROWTH IN LAMBS [J].