STRUCTURE AND SOLID-STATE SN-119 AND TE-125 NMR-SPECTRA OF 2,2,4,4,6,6-HEXAKIS(TRIMETHYLSILYLMETHYL)CYCLOTRISTANNATELLURANE

被引：3

作者：

EINSTEIN, FWB

GAY, ID

JONES, CHW

RIESEN, A

SHARMA, RD

机构：

[1] Department of Chemistry, Simon Fraser University, Burnaby, V5A1S5, BC

来源：

ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS | 1993年 / 49卷

关键词：

D O I：

10.1107/S0108270192008400

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

{[(CH3)3SiCH2]2SnTe}3, C24H66Si6Sn3Te3, M(r) = 1262.2, monoclinic, P2(1)/c, a = 18.392 (3), b = 12.7234 (3), c = 22.183 (3) angstrom, beta = 107.86 (2)-degrees, V = 4941 angstrom3, Z = 4, D(x) = 1.698 g cm-3, lambda(Mo Kalpha) = 0.71069 angstrom, mu = 34.14 cm-1, F(000) = 2399.8, T = 293 K, R = 0.047 for 2480 observed reflections. The molecule has a twist-boat conformation similar to that of [(CH3)3SnTe]3. The solid-state Sn-119 and Te-125 NMR parameters are briefly discussed.

引用

页码：470 / 472

页数：3

共 9 条

[1] 2 CRYSTAL MODIFICATIONS OF HEXAMETHYLCYCLOTRISTANNATELLURANE [J].