SUPERCRITICAL-FLUID EXTRACTION OF FLUVALINATE RESIDUES IN HONEY - DETERMINATION BY HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY

被引：32

作者：

ATIENZA, J ^{[1
]}

JIMENEZ, JJ ^{[1
]}

BERNAL, JL ^{[1
]}

MARTIN, MT ^{[1
]}

机构：

[1] FAC SCI VALLADOLID,DEPT ANALYT CHEM,VALLADOLID,SPAIN

来源：

JOURNAL OF CHROMATOGRAPHY A | 1993年 / 655卷 / 01期

关键词：

D O I：

10.1016/0021-9673(93)87016-F

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

A method for the analysis of fluvalinate residues in honey from beehives treated with this product to prevent varroatosis is described. The method involves-supercritical fluid extraction with carbon dioxide and further analysis by high-performance liquid chromatography on a C-18 reversed-phase column, acetonitrile-water (80:20) as mobile phase and detection at 254 nm. This method is simpler than the one in which extraction with organic solvents, thin-layer chromatography and gas chromatography is used.

引用

页码：95 / 99

页数：5

共 15 条

[1] CLEANUP OF COMPLEX ORGANIC MIXTURES USING SUPERCRITICAL FLUIDS AND SELECTIVE ADSORBENTS
ALEXANDROU, N
LAWRENCE, MJ
PAWLISZYN, J
[J]. ANALYTICAL CHEMISTRY, 1992, 64 (03) : 301 - 311
[2] AVILA C, 1990, VIDA APICOLA, V44, P14
[3] DETERMINATION OF RESIDUES OF SYNTHETIC PYRETHROIDS IN FRUIT AND VEGETABLES BY GAS-LIQUID AND HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY
BAKER, PG
BOTTOMLEY, P
[J]. ANALYST, 1982, 107 (1271) : 206 - 212
[4] BORNECK R, 1989, REV FRANCAISE APICUL, V485, P228
[5] DETERMINATION OF FLUVALINATE METABOLITE RESIDUES IN COTTONSEED, APPLES, TOMATOES, AND SOIL
FITCH, WL
SJOLANDER, AC
MILLER, WW
[J]. JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 1988, 36 (04) : 764 - 766
[6] FITCH WL, 1984, ANAL METHODS PESTICI, V13, P79
[7] HAOVAR M, 1990, AGRONOMIE, V2, P133
[8] HOPPER ML, 1991, J ASSOC OFF ANA CHEM, V74, P234
[9] KHAZANCHI R, 1989, J ASSOC OFF ANA CHEM, V72, P512
[10] MILLER DJ, 1992, ANAL CHEM, V64, P405

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