APPARATUS FOR THE IN-SITU KINETIC-STUDY OF REACTIONS INVOLVING AIR SENSITIVE MATERIALS USING ENERGY-DISPERSIVE POWER DIFFRACTION

被引：22

作者：

CLARK, SM ^{[1
]}

IRVIN, P ^{[1
]}

FLAHERTY, J ^{[1
]}

RATHBONE, T ^{[1
]}

WONG, HV ^{[1
]}

EVANS, JSO ^{[1
]}

OHARE, D ^{[1
]}

机构：

[1] UNIV OXFORD,RADIOL SCI LAB,OXFORD OX1 3QR,ENGLAND

来源：

REVIEW OF SCIENTIFIC INSTRUMENTS | 1994年 / 65卷 / 07期

关键词：

D O I：

10.1063/1.1144729

中图分类号：

TH7 [仪器、仪表];

学科分类号：

0804 ; 080401 ; 081102 ;

摘要：

A novel sample chamber has been developed for the study of chemical reactions involving air sensitive samples using energy-dispersive powder diffraction. The apparatus consists of a reaction vessel, automatic reactant dispensing system, heating jacket, stirrer, and gas purge system. The use of this apparatus is illustrated with data collected on station 9.7 of the UK Synchrotron Radiation Source during a study on the intercalation of cobaltocene into tin disulfide.

引用

页码：2210 / 2213

页数：4

共 10 条

[1]

ACRIVOS JV, 1975, J PHYS CHEM-US, V79, P3003, DOI 10.1021/j100593a043

[2]

Bamford CH, 1980, REACTIONS SOLID STAT

[3] A 2-STEP MODEL OF INTERCALATION [J].