EVALUATION OF A 13.56 MHZ CAPACITIVELY COUPLED PLASMA AS A DETECTOR FOR GAS-CHROMATOGRAPHIC DETERMINATION OF ORGANOTIN COMPOUNDS

被引:27
作者
HUANG, DG [1 ]
BLADES, MW [1 ]
机构
[1] UNIV BRITISH COLUMBIA,DEPT CHEM,2036 MAIN MALL,VANCOUVER V6T 1Y6,BC,CANADA
关键词
CAPACITIVELY COUPLED PLASMA; GAS CHROMATOGRAPHY; ORGANOTIN COMPOUNDS;
D O I
10.1039/ja9910600215
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
A demountable, parallel plate, capacitively coupled plasma source operating at 13.56 MHz has been developed as a gas-chromatographic detector for the determination of organotin compounds. The effect of operating power and gas flow-rate on analyte emission intensity has been measured and spatial emission characteristics of the plasma have been evaluated. The detection limits for Me4Sn, Me3SnCl and Pr4Sn were 0.079, 0.190 and 0.168 ng s-1, respectively.
引用
收藏
页码:215 / 219
页数:5
相关论文
共 20 条
[1]   SELECTIVE EMISSION SPECTROMETRIC DETERMINATION OF NANOGRAM QUANTITIES OF ORGANIC BROMINE CHLORINE IODINE PHOSPHORUS AND SULFUR COMPOUNDS IN A HELIUM PLASMA [J].
BACHE, CA ;
LISK, DJ .
ANALYTICAL CHEMISTRY, 1967, 39 (07) :786-&
[2]   EFFECTS OF DOPANTS ON TIN EMISSION IN A HELIUM MICROWAVE-INDUCED PLASMA [J].
BESNER, A ;
HUBERT, J .
JOURNAL OF ANALYTICAL ATOMIC SPECTROMETRY, 1988, 3 (02) :381-385
[3]  
CROMPTON TR, 1981, COMPREHENSIVE ORGANO, P487
[4]  
ESTES SA, 1981, ANAL CHEM, V53, P133
[5]   SPECIATION OF INORGANIC AND ORGANOMETALLIC COMPOUNDS IN SOLID BIOLOGICAL SAMPLES BY THERMAL VAPORIZATION AND PLASMA EMISSION-SPECTROMETRY [J].
HANAMURA, S ;
SMITH, BW ;
WINEFORDNER, JD .
ANALYTICAL CHEMISTRY, 1983, 55 (13) :2026-2032
[6]   CAPACITIVELY COUPLED PLASMA DETECTOR FOR GAS-CHROMATOGRAPHY [J].
HUANG, DG ;
LIANG, DC ;
BLADES, MW .
JOURNAL OF ANALYTICAL ATOMIC SPECTROMETRY, 1989, 4 (08) :789-791
[7]   NEW MICROWAVE PLASMA AT ATMOSPHERIC-PRESSURE [J].
HUBERT, J ;
MOISAN, M ;
RICARD, A .
SPECTROCHIMICA ACTA PART B-ATOMIC SPECTROSCOPY, 1979, 34 (01) :1-10
[8]   TRACE ANALYSIS AND SPECIATION FOR METHYLATED ORGANOTINS BY HPLC-HYDRIDE GENERATION-DIRECT CURRENT PLASMA EMISSION-SPECTROSCOPY (HPLC-HY-DCP) [J].
KRULL, IS ;
PANARO, KW .
APPLIED SPECTROSCOPY, 1985, 39 (06) :960-967
[9]  
MCCORMACK AJ, 1965, ANAL CHEM, V37, P147
[10]  
Pearse RWB, 1976, IDENTIFI CATION MOL, V4th, DOI DOI 10.1007/978-94-009-5758-9