EVOLVED GAS-ANALYSIS OF INORGANIC-COMPOUNDS WITH A QUADRUPOLE MASS-SPECTROMETER COUPLED TO A THERMOGRAVIMETRIC ANALYZER

被引:23
作者
LESKELA, T
LIPPMAA, M
NIINISTO, L
SOININEN, P
机构
[1] Laboratory of Inorganic and Analytical Chemistry, Helsinki University of Technology
关键词
D O I
10.1016/0040-6031(93)80031-5
中图分类号
O414.1 [热力学];
学科分类号
摘要
An inexpensive EGA system, based on a quadrupole MS and a standard PC, has been constructed and connected to a commercial thermobalance via a heated capillary. The system has been tested with various inorganic compounds including CaC2O4. H2O, CuSO4. 5H2O, Cu(NH3)4SO4. H2O and [Pt(NH3)5OH]Cl3. H2O. The applicability of the TG-EGA-MS system is discussed.
引用
收藏
页码:9 / 18
页数:10
相关论文
共 37 条
[1]   APPLICATIONS OF NEW METHODS AND INSTRUMENTATION IN THERMAL-ANALYSIS [J].
BARNES, PA .
THERMOCHIMICA ACTA, 1987, 114 (01) :1-13
[2]   THERMOGRAVIMETRY COMBINED WITH CHEMICAL IONIZATION MASS-SPECTROMETRY A NEW TECHNIQUE IN THERMAL-ANALYSIS [J].
BAUMGARTNER, E ;
NACHBAUR, E .
THERMOCHIMICA ACTA, 1977, 19 (01) :3-12
[3]  
CARANGELO RM, 1990, AM LAB, V20, P51
[4]   A NEW INTEGRATED SYSTEM FOR SIMULTANEOUS TG-DTA-MASS SPECTROMETRY [J].
CHARSLEY, EL ;
MANNING, NJ ;
WARRINGTON, SB .
THERMOCHIMICA ACTA, 1987, 114 (01) :47-52
[5]  
CHARSLEY EL, 1990, AM LAB, V20, P21
[6]   POLYMER CHARACTERIZATION BY COUPLED THERMOGRAVIMETRY-GAS CHROMATOGRAPHY [J].
CHIU, J .
ANALYTICAL CHEMISTRY, 1968, 40 (10) :1516-&
[7]   A LIMITED BUDGET APPROACH TO TG-MS [J].
CLARKE, E .
THERMOCHIMICA ACTA, 1981, 51 (01) :7-15
[8]  
CODY CA, 1991, AM LAB, V13, P93
[9]  
Collins L. W., 1974, THERMOCHIM ACTA, V9, P15
[10]   MASS-SPECTROMETRIC EVOLVED GAS-ANALYSIS - AN OVERVIEW [J].
DOLLIMORE, D ;
GAMLEN, GA ;
TAYLOR, TJ .
THERMOCHIMICA ACTA, 1984, 75 (1-2) :59-69