2-STAGE DERIVATIZATION WITH N-(TERT-BUTYLDIMETHYLSILYL)-N-METHYL-TRIFLUOROACETAMIDE (MTBSTFA) AND N-METHYL-BIS-(TRIFLUOROACETAMIDE) (MBTFA) FOR THE GAS-CHROMATOGRAPHIC ANALYSIS OF OH-COMPOUNDS, SH-COMPOUNDS AND NH-COMPOUNDS

被引：24

作者：

SCHOENE, K

BRUCKERT, HJ

STEINHANSES, J

KONIG, A

机构：

[1] Fraunhofer-Institut für Umweltchemie und Ökotoxikologie, Schmallenberg, D-57377

来源：

FRESENIUS JOURNAL OF ANALYTICAL CHEMISTRY | 1994年 / 348卷 / 5-6期

关键词：

D O I：

10.1007/BF00323136

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

Various alcohols, thiols, phenols, carboxylic acids, amines and amides were subjected to silylation with MTBSTFA followed by trifluoroacetylation with MBTFA. The reaction products have been identified and quantified by means of gas chromatography coupled with atomic emission and mass spectrometric detection.

引用

页码：364 / 370

页数：7

共 16 条

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