REDUCTION OF MATRIX INTERFERENCES AND IMPROVEMENT OF DETECTION POWER IN FLAME AAS BY A HIGH-PERFORMANCE FLOW HYDRAULIC HIGH-PRESSURE NEBULIZATION SYSTEM FOR SAMPLE INTRODUCTION (HPF/HHPN) - TRACE-ELEMENT DETERMINATION IN ALUMINUM, IRON AND COPPER

被引:23
作者
BERNDT, H
MULLER, A
机构
[1] Institut für Spektrochemie und angewandte Spektroskopie, Dortmund 1, W-4600
来源
FRESENIUS JOURNAL OF ANALYTICAL CHEMISTRY | 1993年 / 345卷 / 01期
关键词
D O I
10.1007/BF00323320
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
For analysis of highly concentrated salt solutions, the samples are injected into a high-performance carrier stream and transported to a special high-pressure nebulization nozzle (max. pressure: 400 bar/40 MPa). An aerosol of very small droplets is formed only by the high fluid pressure without using nebulization gas. The nozzle replaces the pneumatic nebulizer (high-performance flow/hydraulic high-pressure nebulization system: HPF/HHPN). In comparison with pneumatic nebulization, matrix interferences are significantly reduced and sensitivity is improved by factors of 2 to 8 (depending on the element and matrix to be analyzed). For the determination of 10 elements in the matrices Al (30 g/l), Fe (150 g/l) and Cu (330 g/l), the element-specific improvement of the detection power by a factor of 4.1 to 9.7 for Al, 1.3 to 4.9 for Fe and 1.3 to 10 for Cu is achieved.
引用
收藏
页码:18 / 24
页数:7
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