SPECTROFLUOROMETRIC FLOW-INJECTION DETERMINATION OF ADRENALINE WITH AN IODINE SOLID-PHASE REACTOR

被引：25

作者：

KOJLO, A ^{[1
]}

CALATAYUD, JM ^{[1
]}

机构：

[1] UNIV VALENCIA,DEPT QUIM ANALIT,E-46100 BURJASSOT,SPAIN

来源：

ANALYTICA CHIMICA ACTA | 1995年 / 308卷 / 1-3期

关键词：

FLOW INJECTION; FLUOROMETRY; ADRENALINE HYDROCHLORIDE; PHARMACEUTICAL ANALYSIS;

D O I：

10.1016/0003-2670(94)00656-7

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

A novel strategy for the preparation of solid-phase reactors by ''impregnation'' of a poly(vinyl chloride) coil with the reagent was carried out and applied to the fluorimetric flow injection determination of adrenaline. The calibration graph was linear over the range 5-25 mg l(-1) of adrenaline, the reproducibility (R.S.D.) was 1.8% (15 replicates) and the sample throughput 32 h(-1).

引用

页码：334 / 338

页数：5

共 11 条

[1]

FLorey K., 1981, ANAL PROFILES DRUG S, V10

[2] THE CHEMISTRY OF ADRENOCHROME AND ITS DERIVATIVES [J].