SUPERCRITICAL FLUID FRACTIONATION OF PETROLEUM-DERIVED AND COAL-DERIVED MIXTURES

被引:52
作者
CAMPBELL, RM [1 ]
LEE, ML [1 ]
机构
[1] BRIGHAM YOUNG UNIV,DEPT CHEM,PROVO,UT 84602
关键词
CHROMATOGRAPHIC ANALYSIS - Column - ORGANIC COMPOUNDS - Chromatographic Analysis;
D O I
10.1021/ac00124a028
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
A supercritical fluid chromatographic system was constructed to provide separations and fraction collection on a semipreparative scale. Columns packed with silica materials of intermediate particle sizes (30-70 mu m) were used to allow dynamic pressure programming with minimum pressure drop of the CO//2 mobile phase along the length of the column. A variety of complex coal- and petroleum-derived polycyclic aromatic compound mixtures were fractionated according to the number of aromatic rings using columns packed with an NH//2-modified stationary phase bonded on silica particles.
引用
收藏
页码:2247 / 2251
页数:5
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