THE STEREOCHEMICAL INVESTIGATION OF 3-ARYL-4-METHYL-1,2,3-OXATHIAZOLIDINE 2-OXIDES USING NMR

被引：4

作者：

NISHIYAMA, T

TAKAHAMA, Y

YAMADA, F

机构：

[1] Department of Applied Chemistry, Faculty of Engineering, Kansai University, Suita, Osaka, 564, Senriyama

来源：

JOURNAL OF HETEROCYCLIC CHEMISTRY | 1990年 / 27卷 / 02期

关键词：

D O I：

10.1002/jhet.5570270215

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

The title compounds were prepared by the reaction of the corresponding N‐2‐hydroxyisopropylanilines with thionyl chloride in the presence of triethylamine, and their pmr and cmr spectra were examined. On the basis of the chemical shifts due to the γ‐ and δ‐effects, the stereochemical structures are discussed. Copyright © 1990 Journal of Heterocyclic Chemistry

引用

收藏

页码：195 / 197

页数：3

相关论文

共 12 条

[1]

ALLINGER NL, 1965, CONFORMATIONAL ANAL, P437

[2]

ANTEUNIS M, 1964, B SOC CHIM BELG, V73, P889

[3] DOWNFIELD-DELTA STERIC SHIFTS IN C-13 NMR OF ACYCLIC MOLECULES [J].

BATCHELOR, JG .

JOURNAL OF MAGNETIC RESONANCE, 1975, 18 (01) :212-214

[4]

BUCHANAN GW, 1978, TETRAHEDRON LETT, P2775

[5] APPLICATION OF C-13 NUCLEAR MAGNETIC-RESONANCE TO CONFORMATIONAL-ANALYSIS OF TRIMETHYLENE SULFITES .36. [J].

BUCHANAN, GW ;

STOTHERS, JB ;

WOOD, G .

CANADIAN JOURNAL OF CHEMISTRY-REVUE CANADIENNE DE CHIMIE, 1973, 51 (22) :3746-3751

[6] CHEMISTRY OF S=O BOND .4. CONFORMATIONAL-ANALYSIS OF ETHYLENE SULFITES [J].

GREEN, CH ;

HELLIER, DG .

JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 2, 1975, (03) :190-193

[7] STEREOCHEMICAL DEPENDENCE OF DELTA-SUBSTITUENT EFFECTS IN C-13 NMR-SPECTRA - DESHIELDING SYN-AXIAL INTERACTIONS [J].

GROVER, SH ;

GUTHRIE, JP ;

STOTHERS, JB ;

TAN, CT .

JOURNAL OF MAGNETIC RESONANCE, 1973, 10 (02) :227-230

[8] NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY . EFFECTS OF MOLECULAR ASYMMETRY ON CARBON-13 CHEMICAL SHIFTS [J].

KROSCHWITZ, JI ;

WINOKUR, M ;

REICH, HJ ;

ROBERTS, JD .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1969, 91 (21) :5927-+

[9] STEREOCHEMISTRY OF 5-SUBSTITUTED 2-OXO-3-ARYL-1,2,3-OXATHIAZOLIDINES [J].

NISHIYAMA, T ;

YAMADA, F .

BULLETIN OF THE CHEMICAL SOCIETY OF JAPAN, 1971, 44 (11) :3073-+

[10] PROTON MAGNETIC RESONANCE, STRUCTURE AND STEREOISOMERISM IN CYCLIC SULFITES [J].

PRITCHARD, J ;

LAUTERBUR, PC .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1961, 83 (09) :2105-&