PREPARATION AND CHARACTERIZATION OF UNIFORM SUBMICROMETER METAL NIOBATE PARTICLES .1. LEAD NIOBATE

被引:21
作者
KIM, MJ [1 ]
MATIJEVIC, E [1 ]
机构
[1] CLARKSON UNIV,DEPT CHEM ENGN,POTSDAM,NY 13699
关键词
Chemical Reactions - Reaction Kinetics - Metallic Compounds - Chelation - Organometallics - Decomposition;
D O I
10.1557/JMR.1991.0840
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Collodial amorphous lead niobate particles of different composition and morphologies were obtained by a metal-chelate decomposition method. The nature of the dispersions depended on the conditions of the preparation of the complexes, pH, aging time, and temperature. The structural and chemical changes of the so prepared powders on calcination were investigated by thermal and x-ray diffraction analyses. Chemical mechanisms of the formation and transformation of the particles are suggested.
引用
收藏
页码:840 / 850
页数:11
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