RELATIVE SIGN DETERMINATION OF PHOSPHORUS CARBON COUPLING-CONSTANTS BY 2D C-13 NMR-SPECTROSCOPY

被引：14

作者：

RANDALL, LH ^{[1
]}

CHERKAS, AA ^{[1
]}

CARTY, AJ ^{[1
]}

机构：

[1] UNIV WATERLOO,GUELPH WATERLOO CTR GRAD WORK CHEM,DEPT CHEM,WATERLOO CAMPUS,WATERLOO N2L 3G1,ONTARIO,CANADA

来源：

ORGANOMETALLICS | 1989年 / 8卷 / 02期

关键词：

D O I：

10.1021/om00104a051

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

引用

页码：568 / 571

页数：4

共 22 条

[1]

ALLMAN T, 1987, J MAGN RESON, V86, P533

[2] FOURIER-TRANSFORM HETERONUCLEAR MAGNETIC TRIPLE RESONANCE IN COMPLEX SPIN SYSTEMS .3. SYMMETRICAL DITERTIARY PHOSPHINE COMPLEXES OF GROUP-VI METAL-CARBONYLS [J].

ANDREWS, GT ;

COLQUHOUN, IJ ;

MCFARLANE, W .

POLYHEDRON, 1983, 2 (08) :783-790

[3] RELATIVE SIGNS OF NMR SPIN COUPLING-CONSTANTS BY TWO-DIMENSIONAL FOURIER-TRANSFORM SPECTROSCOPY [J].

BAX, A ;

FREEMAN, R .

JOURNAL OF MAGNETIC RESONANCE, 1981, 45 (01) :177-181

[4] CORRELATION OF PROTON CHEMICAL-SHIFTS BY TWO-DIMENSIONAL FOURIER-TRANSFORM NMR [J].

BAX, A ;

FREEMAN, R ;

MORRIS, G .

JOURNAL OF MAGNETIC RESONANCE, 1981, 42 (01) :164-168

[5]

BAX A, 1982, 2 DIMENSIONAL NMR LI

[6] RAPID ACCESS TO W-183 NMR PARAMETERS OF TUNGSTEN COMPLEXES VIA REVERSE 2D H-1,W-183 AND P-31,W-183 NMR-SPECTROSCOPY [J].

BENN, R ;

BRENNEKE, H ;

HECK, J ;

RUFINSKA, A .

INORGANIC CHEMISTRY, 1987, 26 (17) :2826-2829

[7] A TRIAD OF ELECTRON-RICH MU2-ALKYLIDENE COMPLEXES M2(CO)6[MU-CHC(PH)NET2](MU-PPH2)(M=FE,RU,OS) VIA THE ADDITION OF DIETHYLAMINE TO THE ACETYLIDES M2(CO)6(MU2-ETA-2-C=CPH)(MU-PPH2) - SPECTROSCOPIC PROPERTIES AND STRUCTURAL CHEMISTRY [J].

CHERKAS, AA ;

MOTT, GN ;

GRANBY, R ;

MACLAUGHLIN, SA ;

YULE, JE ;

TAYLOR, NJ ;

CARTY, AJ .

ORGANOMETALLICS, 1988, 7 (05) :1115-1121

[8] UNSYMMETRICAL BISPHOSPHORUS LIGANDS .14. MULTI-NUCLEAR MAGNETIC-RESONANCE STUDIES OF GROUP-6 METAL-CARBONYL-COMPLEXES OF UNSYMMETRICAL BISPHOSPHORUS LIGANDS [J].

COLQUHOUN, IJ ;

GRIM, SO ;

MCFARLANE, W ;

MITCHELL, JD ;

SMITH, PH .

INORGANIC CHEMISTRY, 1981, 20 (08) :2516-2521

[9] DETERMINATION OF THE RELATIVE SIGNS OF 2J(P-31-P-31) IN COMPLEXES OF TUNGSTEN(O) AND MOLYBDENUM(O) USING TWO-DIMENSIONAL [P-31-P-31]-COSY-45 NUCLEAR-MAGNETIC-RESONANCE CHEMICAL-SHIFT CORRELATION [J].

FONTAINE, XLR ;

KENNEDY, JD ;

SHAW, BL ;

VILA, JM .

JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS, 1987, (10) :2401-2405

[10] C-13 NMR CHEMICAL-SHIFT TENSORS OF METAL-CARBONYLS [J].

GLEESON, JW ;

VAUGHAN, RW .

JOURNAL OF CHEMICAL PHYSICS, 1983, 78 (09) :5384-5392

← 1 2 3 →