PREPARATION AND CRYSTAL-STRUCTURE OF (CH3NH3)8[NDCL6][NDCL4(H2O)2]2CL3

被引:13
作者
RUNGE, P [1 ]
SCHULZE, M [1 ]
URLAND, W [1 ]
机构
[1] UNIV HANOVER,INST ANORGAN CHEM,CALLINSTR 9,W-3000 HANNOVER 1,GERMANY
来源
ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE | 1991年 / 592卷 / 01期
关键词
OCTAMETHYLAMMONIUM TRICHLORIDE BIS(DIAQUATETRACHLORONEODYMATE HEXACHLORONEO; SINGLE CRYSTAL STRUCTURE; PREPARATION;
D O I
10.1002/zaac.19915920113
中图分类号
O61 [无机化学];
学科分类号
070301 ; 081704 ;
摘要
[CH3NH3)8[NdCl6][NdCl4(H2O)2]2Cl3 is for the first time prepared and investigated by X-ray, single crystal work. It crystallizes in the monoclinic system (space group C2/m, Z = 2) with a = 9.358(5), b = 17.424(9), c = 15.360(8) angstrom, beta = 108.30(4)-degrees. The structure contains besides isolated Cl- ions distorted [NdCl6]3- octahedra and [NdCl4(H2O)2]- chains.
引用
收藏
页码:115 / 120
页数:6
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