SOLID-LIQUID PHASE-TRANSFER CATALYTIC SYNTHESIS .10. THE RAPID ALKYLATION OF ETHYL ACETOACETATE UNDER MICROWAVE IRRADIATION

被引：18

作者：

DENG, RH ^{[1
]}

WANG, YL ^{[1
]}

JIANG, YZ ^{[1
]}

机构：

[1] ACAD SINICA,CHENGDU INST ORGAN CHEM,CHENGDU 610041,PEOPLES R CHINA

来源：

SYNTHETIC COMMUNICATIONS | 1994年 / 24卷 / 01期

基金：

中国国家自然科学基金;

关键词：

Microwave irradiation - Synthesis (chemical);

D O I：

10.1080/00397919408012633

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Rapid alkylation of ethyl acetoacetate with a series of halides were performed in 650W domestic microwave oven and the isolated yield of monoalkylated product varying from 59 to 82%.

引用

页码：111 / 115

页数：5

共 6 条

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