ASSIGNMENTS OF THE H-1 AND C-13 NMR-SPECTRA OF TRANS-4-HYDROXY-N-9-FLUORENYLMETHOXYCARBONYL-L-PROLINE - USING ONE-DIMENSIONAL AND 2-DIMENSIONAL NMR-SPECTROSCOPY

被引：1

作者：

AKSNES, DW ^{[1
]}

FRANCIS, GW ^{[1
]}

PAPAIOANNOU, D ^{[1
]}

机构：

[1] UNIV PATRAS,DEPT CHEM,PATRAI,GREECE

来源：

MAGNETIC RESONANCE IN CHEMISTRY | 1993年 / 31卷 / 09期

关键词：

H-1; NMR; C-13; PROLINE DERIVATIVES; CONFORMATION;

D O I：

10.1002/mrc.1260310916

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The H-1 and C-13 NMR spectra of trans-4-hydroxy-N-9-fluorenylmethoxycarbonyl-L-proline show a 56:44 mixture of two conformers due to hindered rotation around the partial C-N double bond. A combination of homo- and heteronuclear 1 D and 2D NMR techniques provided the assignments of the H-1 and C-13 resonances.

引用

页码：876 / 877

页数：2

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